data = {{x1,R1},{x2,R2},{x3,R3}...,{xm,Rm}};
loglog=Function[{x,y},{Log[x/[Ca2+]0],Log[y]}];
datalog=Apply[loglog,data,{1}];


peakr = Function[{A,B,C,x},Piecewise[{{A+(1/2)*Log[1-(2/3)*Bx]
+C*(1-(1-(2/3)*Bx)^(3/2),x<3/2/B,Infinity}}]];


fit = NonlinearModelFit[datalog,{peakr[A,B,C,x],{A>0,B>0,C>0}},
{{A,A0},{B,B0},{C,C0}},x,Method->NMinimize];
fit['ParameterTable']
  1. Table with Code Blocks